Experimental Assessment of the Influence of Colloid Migration on the Filtration Characteristics of Carbonate Rocks under Cyclic Loading

Evgenii P. Riabokon, Ahmad Farid Bin Abu Bakar, Khairul Azlan Mustapha, Daniil E. Katunin, Yan V. Savitsky, Liyuan Yu, Aleksei G. Parshakov

Author details

Evgenii P. Riabokon
Perm National Research Polytechnic University, Perm, Russian Federation
Ahmad Farid Bin Abu Bakar
University of Malaya, Kuala Lumpur, Malaysia
Khairul Azlan Mustapha
University of Malaya, Kuala Lumpur, Malaysia
Daniil E. Katunin
Perm National Research Polytechnic University, Perm, Russian Federation
Yan V. Savitsky
Perm National Research Polytechnic University, Perm, Russian Federation
Liyuan Yu
China University of Mining and Technology, Xuzhou, China
Aleksei G. Parshakov
Perm National Research Polytechnic University, Perm, Russian Federation

https://doi.org/10.15593/2712-8008/2025.3.11

The influence of natural colloidal particle migration on changes in the permeability of carbonate reservoirs under transient and cyclic loading is considered. To exclude chemical and plastic factors, an experimental technique was developed based on the saturation and drying of cores with isopropyl alcohol as an inert fluid. The studies were conducted on carbonate cores with different porosity and initial permeability. It was shown that after saturation and drying cycles, the permeability of individual samples either decreases or increases depending on the nature of colloid migration: blocking or clearing of pore channels. It was determined that the maximum permeability values in the loading cycle reflect the true permeability of the rock, at which the effect of colloidal migration is minimal. Based on the obtained data, power-law dependences of relative permeability on effective pressure with high correlation coefficients (R2 > 0.99) were constructed, which allows us to isolate the elastic component of changes in filtration properties. A comparison of water-saturated experiments revealed a significant effect of mineral dissolution (calcite, halite, etc.) on the increase in apparent permeability. Microscopic and tomographic analysis confirmed the preservation of the overall structure, but also revealed localized colloid redistribution, similar to the "coffee ring" effect. The developed methodology provides a quantitative assessment of the contribution of colloid migration to permeability hysteresis and can be used to refine reservoir flow-mechanical models, improving the accuracy of reservoir performance predictions.

Keywords

permeabilitycolloid migrationcarbonate reservoirspermeability hysteresisfiltration propertieseffective pressure

Экспериментальная оценка влияния миграции коллоидов на фильтрационные характеристики карбонатных пород при циклическом нагружении

Рассматривается влияние миграции естественных коллоидных частиц на изменение проницаемости карбонатных коллекторов при нестационарных и циклических нагрузках. Для исключения химических и пластических факторов разработана экспериментальная методика, основанная на насыщении и сушке кернов изопропиловым спиртом как инертным флюидом. Исследования проведены на карбонатных кернах с различной пористостью и начальной проницаемостью. Показано, что после циклов насыщения и сушки проницаемость отдельных образцов либо снижается, либо возрастает в зависимости от характера перемещения коллоидов: блокирования или очистки поровых каналов. Определено, что максимальные значения проницаемости в цикле нагружения отражают истинную проницаемость породы, при которой эффект коллоидной миграции минимален. На основе полученных данных построены степенные зависимости относительной проницаемости от эффективного давления с высокими коэффициентами корреляции (R2 > 0,99), что позволяет выделить упругую составляющую изменений фильтрационных свойств. Сравнение экспериментов с насыщением водой выявило существенное влияние растворения минералов (кальцита, галита и др.) на рост кажущейся проницаемости. Микроскопический и томографический анализ подтвердили сохранность общей структуры, однако зафиксировали локальное перераспределение коллоидов, аналогичное эффекту «кофейных колец». Разработанная методика обеспечивает количественную оценку вклада коллоидной миграции в гистерезис проницаемости и может использоваться для уточнения фильтрационно-механических моделей коллекторов, повышая точность прогноза их поведения при эксплуатации.

Ключевые слова

проницаемостьмиграция коллоидовкарбонатные коллекторыгистерезис проницаемостифильтрационные свойстваэффективное давление

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16.Civan. F. Parameterization of Biot–Willis Effective-Stress Coefficient for Deformation and Alteration of Porous Rocks / F. Civan // Transp Porous Media. – 2021. – Т. 138, № 2. – С. 337–368. Scholar
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42.The Stress‐Memory Effect of Fracture Stiffness During Cyclic Loading in Low‐Permeability Sandstone / C. Kluge [и др.] // J Geophys Res Solid Earth. – 2021. – Т. 126, № 10. Scholar
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Article information

Published: 24 October 2025
Issue date: 24 October 2025
Issue: Vol. 25, No. 3 (2025)